Synthesis of ethyl 3-oxo-2-(3,4,5-trifluoro-2,6-dimethoxybenzoyl)butyrate

Autor: Kisil', S., Kodess, M., Burgart, Ya., Saloutin, V.
Zdroj: Russian Chemical Bulletin; June 2000, Vol. 49 Issue: 6 p1090-1092, 3p
Abstrakt: Abstract: Ethyl acetoacetate was acylated with 3,4,5-trifluoro-2,6-dimethoxybenzoyl chloride to give, for the first time, ethyl 3-oxo-2-(3,4,5-trifluoro-2,6-dimethoxybenzoyl)butyrate and its copper chelate. The title compound was used for the synthesis of 6,7,8-trifluoro-5-hydroxy-2-methylchromone, 1-(3,4,5-trifluoro-2,6-dimethoxyphenyl)butane-1,3-dione, and its copper chelate.
Databáze: Supplemental Index