| Autor: |
González Gigosos, P., Fente Sampayo, C., Franco Abuín, C., Vázquez Belda, B., Quinto Fernández, E., Cepeda Sáez, A. |
| Zdroj: |
Chromatographia; September 1996, Vol. 43 Issue: 5-6 p271-274, 4p |
| Abstrakt: |
This paper reports a method employing diphasic dialysis extraction for the rapid confirmation of clenbuterol in cow liver by RPHPLC with diode-array detection. The most suitable means of homogenizing the liver is in barium hydroxide-barium chloride buffer; the optimum extraction solvent istert-butyl methyl ether at an extraction temperature of 37°C; stirring should be applied at 150 r.p.m. for 4h. This extraction method improves clenbuterol recovery values to 98.9%. |
| Databáze: |
Supplemental Index |
| Externí odkaz: |
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