Schnelle Bestimmung von Furfurol und Hydroxymethylfurfurol in alkoholischen Getränken mit Hilfe der Umkehrphasen-Chromatographie

Autor: Frischkorn, Hanna E., Wanderley-Casado, Martha, Frischkorn, Claus G. B.
Zdroj: Zeitschrift für Lebensmitteluntersuchung und -Forschung A; March 1982, Vol. 174 Issue: 2 p117-121, 5p
Abstrakt: Summary Furfural and Hydroxymethylfurfural can easily be determined in alcoholic beverages by means of reverse phase chromatography. A special sample preparation is not necessary. The aldehydes are detected by UV-spectrometry, the absolute detection limit in routine work is 4–7 mg/100 liters of pure ethanol (corresponding to 0.016–0.03 mg/l beverage) and can be extended down to 0.002–0.001 mg/l when injecting higher volumes for trace analysis. In the range of 0.25–3 mg/l linear relationship is obtained between peak hight and concentration. The complete assay procedure takes about 12 min. A series of Brazilian Cachaça samples and German commercial liquors were investigated with the here described method.
Databáze: Supplemental Index