Acylation of aliphatic diamines with methyl nitroacetate

Autor: Lyapkalo, I. M., Ioffe, S. L., Strelenko, Yu. A., Tartakovsky, V. A.
Zdroj: Russian Chemical Bulletin; September 1996, Vol. 45 Issue: 9 p2245-2247, 3p
Abstrakt: N,N'-Bis(nitroacetyl)diamines were synthesized for the first time by the reaction of methyl nitroacetate with aliphatic diamines in H2O or EtOH in the presence of pyridine or imidazole. In the case of 1,2-ethylenediamine, theN-mononitroacetyl derivative was isolated as an intermediate product.
Databáze: Supplemental Index