Synthesis of heterocyclic azoxy compounds from C-nitroheterocyclic compounds and metal derivatives oftert-butylamine
Autor: | Apasov, É. T., Shepelev, E. V., Dzhetigenov, B. A., Strelenko, Yu. A., Kalinin, A. V., Tartakovskii, V. A. |
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Zdroj: | Russian Chemical Bulletin; July 1992, Vol. 41 Issue: 7 p1280-1281, 2p |
Abstrakt: | The reaction of 3-nitropyrazole and 3(5)-nitro-1,2,4-triazole with t-BuNHMgBr gives the corresponding asymmetrical diazene oxides. Furthermore, 3(5)-(1,1-dimethylethyl)azoxy-1,2,4-triazole was also synthesized by the reaction of 1-trimethylsilyl-3(5)-nitro-1,2,4-triazole with t-BuNHLi. |
Databáze: | Supplemental Index |
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