Quantitative determination of nitro-compounds with stannous chloride and fischer reagent in nonaqueous medium

Autor: Dubinskii, R. A., Klimova, V. A.
Zdroj: Russian Chemical Bulletin; July 1970, Vol. 19 Issue: 7 p1396-1400, 5p
Abstrakt: 1.A micromethod of the reduction of nitro-compounds with stannous chloride in nonaqueous medium with stannometric and aquametric ending was developed. The results of the determinations by these two methods of analytical control are in good agreement.2.In nonaqueous medium the reduction of nitroaryls occurs quantitatively, just as in aqueous medium; nitroalkyls are 30% reduced.
Databáze: Supplemental Index