Vitamin B6 analogs

Autor: Karpeiskii, M. Ya., Padyukova, N. Sh., Florent'ev, V. L.
Zdroj: Chemistry of Heterocyclic Compounds; April 1971, Vol. 7 Issue: 4 p465-468, 4p
Abstrakt: 4-Acetyl-3-hydroxy-5-hydroxymethyl-2-methylpyridine 5-phosphate (IV) was synthesized by oxidation of 3-hydroxy-5-hydroxymethyl-4-(a-hydroxyethyl)-2-methylpyridine 5-phosphate (III) with chromic anhydride. Compound III was obtained by phosphorylation of 3-hydroxy-5-hydroxymethyl-4-(a-hydroxyethyl)-2-methylpyridine with polyphosphoric acid (PPA). The UV and PMR spectra of the synthesized compounds were studied.
Databáze: Supplemental Index