Synthesis and crystalline and molecular structure of hydrochloride of 1-[2(2,3-dihydro-1,3,4-oxadiazolyl-5-one)]methyl-7-bromo-5-prenyl-1,2-dihydro-3H-1,4-benzodiazepin-2-one

Autor: Pavlovskii, V. I., Simonov, Yu. A., Dvorkin, A. A., Yavorskii, A. S., Rokachinskaya, M. G., Andronati, S. A.
Zdroj: Chemistry of Heterocyclic Compounds; May 1995, Vol. 31 Issue: 5 p610-614, 5p
Abstrakt: By the interaction of 1-hydrazinocarbonylinethyl-7-bromo-5-phenyl-1,2-dihydro-3H-1,4-benzodiazepin-2-one with phosgene, the compound 1-[2(2,3-dihydro-1, 3,4-oxadiazolyl-5-one)jmethyl-7-bromo-5-phenyl-1, 2-dihydro-3H-1, 4-benzodiazepin-2-one has been synthesized. Spectroscopic methods and x-ray structure analysis have been used to establish the crystalline and molecular structure of this new derivative of 1, 4-benzodiazepine.
Databáze: Supplemental Index
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