The crystal structure of tetraphenylarsonium tricyanooxopyridine-2-carboxylatotungstate(IV) dihydrate

Autor: Leipoldt, Johann G., Basson, Stephen S., Roodt, Andreas, Potgieter, Izak M.
Zdroj: Transition Metal Chemistry; September 1986, Vol. 11 Issue: 9 p323-326, 4p
Abstrakt: The structure of (AsPh4)2[WO(CN)3(Pic)] · 2H2O has been determined from three dimensional x-ray data. The cell dimensions are:a=17.699(8),b=13.546(6),c= 13.590(6) Å, a=117.39(8), ß = 71.54(7) and ? = 115.04(8)°, space group P¯1, Z = 2, The structure was solved from 5279 observed reflections. The anisotropic refinement converged to R = 0.060.
Databáze: Supplemental Index