Autor: |
Yu, Andrew C. C., Mizuno, Mikihisa, Sasaki, Yuichi, Inoue, Makoto, Kondo, Hirofumi, Ohta, Ippei, Djayaprawira, David, Takahashi, Migaku |
Předmět: |
|
Zdroj: |
Applied Physics Letters; 6/16/2003, Vol. 82 Issue 24, p4352, 3p, 2 Diagrams, 2 Graphs |
Abstrakt: |
Monodispersive FePt nanoparticle films can be stabilized firmly on rigid Si substrates using amino-functional silane, such as [3-(2-aminoethlyamino) propyl]trimethoxysilane, as a coupling layer. The Si substrate/SiO[SUB2] /APTS/FePt nanoparticles heterostructure was confirmed using high-resolution electron microscopy (HREM). The HREM result agreed well with the x-ray reflectivity measurement upon the individual layer thickness. The as-made superparamagnetic FePt nanoparticle film transformed from chemically disordered fcc structure to chemically ordered L1[SUB0] phase upon annealing at 800[SUB°]C for 30 min under a vacuum of 10[SUP-8] Torr. Plan-view high-resolution scanning electron microscopy (HRSEM) observation indicated that under high-vacuum annealing, coalescence of the monodispersive nanoparticle film was not significant. The HRSEM result was consistent with the in-plane x-ray diffractometry measurement, in which sharpening of the diffraction peaks occurred only very slightly for the annealed films. [ABSTRACT FROM AUTHOR] |
Databáze: |
Complementary Index |
Externí odkaz: |
|