CHARACTERIZATION OF MATERIAL DEGRADATION IN CERAMIC MATRIX COMPOSITES USING INFRARED REFLECTANCE SPECTROSCOPY.

Autor: Cooney, Adam T., Flattum-Riemers, Richard Y., Scott, Benjamin J.
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Zdroj: AIP Conference Proceedings; 6/23/2011, Vol. 1335 Issue 1, p950-955, 6p, 1 Color Photograph, 2 Graphs
Abstrakt: Ceramic matrix composite materials for thermal protection systems are required to maintain operational performance in extreme thermal and mechanical environments. In-service inspection of materials capable of assessing the degree and extent of damage and degradation will be required to ensure the safety and readiness of future air vehicles. Infrared reflectance spectroscopy is an established material characterization technique capable of extracting information regarding the chemical composition of substances. The viability of this technique as a potentially powerful nondestructive evaluation method capable of monitoring degradation in thermal protection system materials subjected to extreme mechanical and thermal environments is analyzed. Several oxide-based and non-oxide-based ceramic matrix composite materials were stressed to failure in a high temperature environment and subsequently measured using infrared reflectance spectroscopy. Spectral signatures at locations along the length of the samples were compared resulting in distinct and monotonic reflectance peak changes while approaching the fracture point. The chemical significance of the observed signatures and the feasibility of infrared reflectance nondestructive evaluation techniques are discussed. [ABSTRACT FROM AUTHOR]
Databáze: Complementary Index