Lacunary tungstotellurates(iv): [Te2W17O61]12−, [Te2W16O58(OH)2]14−and [Te2W18O62(OH)2]10−Electronic supplementary information (ESI) available: IR data, powder diffraction patterns, cyclic and square wave voltammograms, and experimental details for elemental analysis, NMR spectroscopy, powder diffraction and electrochemistry. For ESI see DOI: 10.1039/c0dt00547a

Autor:	Ritchie, Chris, Alley, Kerwyn G., Boskovic, Colette
Předmět:	VOLTAMMETRY NUCLEAR magnetic resonance spectroscopy ORGANIC chemistry SQUARE waves DIFFRACTION patterns POLYELECTROLYTES
Zdroj:	Dalton Transactions: An International Journal of Inorganic Chemistry; Sep2010, Vol. 39 Issue 38, p8872-8874, 3p
Abstrakt:	A simple procedure is reported for the isolation of the new lacunary tungstotellurate(iv) [Te2W17O61]12−(1a) in multi-gram quantities, with 125Te and 183W NMR spectroscopy indicating retention of the solid state structure in solution. The structurally related polyanions [Te2W16O58(OH)2]14−(2a) and [Te2W18O62(OH)2]10−(2b) were also isolated. [ABSTRACT FROM AUTHOR]
Databáze:	Complementary Index
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