Synthesis and conformation of 6,8,10-trinitro-1,4-dioxaspiro[4.5]decane.

Autor: Atroshchenko, Yu., Golotvin, S., Shakhkel'dyan, I., Shishkin, O., Lavrik, Zh., Borbulevych, O., Antipin, M., Alifanova, E., Gitis, S., Ivanov, I., Kaminsky, A.
Zdroj: Russian Chemical Bulletin; Sep1999, Vol. 48 Issue 9, p1691-1695, 5p
Abstrakt: cis, trans-6,8,10-Trinitro-1,4-dioxaspiro[4.5]decane was synthesized by reduction of the corresponding spirocyclic anionic δ-complex with potassium tetrahydroborate. The molecular structure and the conformation of the title compound were established by X-ray diffraction analysis and1H NMR spectroscopy. [ABSTRACT FROM AUTHOR]
Databáze: Complementary Index