Autor: |
Ban, Irena, Kristl, Matjaž, Volavšek, Bogdan, Golič, Ljubo |
Zdroj: |
Chemical Monthly / Monatshefte für Chemie; Mar1999, Vol. 130 Issue 3, p401-408, 8p |
Abstrakt: |
Crystals of (NH3OH)2TiF6ċ2H2O have been isolated. The compound crystallizes in the monoclinic system (P21/c, No. 15) with cell parameters of a=6.203(1) Å, b=10.057(1) Å, c=7.464(1) Å, and β=110.653(6)°. Reactions in the system In (OH)3– NH3OHF – HF have been investigated. Crystals of (NH3OH)3InF6 were isolated from aqueous solution. The compound crystallizes in the trigonal system (R3c) with a= b= c=7.764(2) Å, α=β=γ=97.21(4)°. The thermal decomposition of both compounds was studied by TG and DSC analysis; the decomposition products were characterized by X-ray powder diffraction. [ABSTRACT FROM AUTHOR] |
Databáze: |
Complementary Index |
Externí odkaz: |
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