Bromination of naphtho[2,3-c][1,2,5]thiadiazole-4,9-dione.

Autor: Konstantinova, L. S., Chechulina, A. S., Obruchnikova, N. V., Knyazeva, E. A., Kan, Bin, Duan, Tainan, Chen, Yongsheng, Rakitin, O. A.
Zdroj: Russian Chemical Bulletin; Oct2024, Vol. 73 Issue 10, p3038-3044, 7p
Abstrakt: Investigations of bromination of naphtho[2,3-c][1,2,5]thiadiazole-4,9-dione revealed that the reaction proceeded most efficiently with N-bromosuccinimide in sulfuric acid and depending on the reaction conditions, can give mono-, di-, tri- and tetrabromo derivatives of naphtho[2,3-c][1,2,5]thiadiazole-4,9-dione. A series of the major isomers was isolated, and their structure was proven using heteronuclear multiple bond correlation NMR spectroscopy and high-resolution mass spectrometry. [ABSTRACT FROM AUTHOR]
Databáze: Complementary Index