| Autor: |
Rameez Khan, Raja Muhammad, Choudhary, Muhammad Aziz, Ahmad, Zahoor, Ibrahim, Mohamad Nasir Mohamad, Adnan, Rohana, Yaqoob, Asim Ali, Rashid, Mohd |
| Předmět: |
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| Zdroj: |
Inorganic & Nano-Metal Chemistry; 2024, Vol. 54 Issue 1, p35-43, 9p |
| Abstrakt: |
Copper oxide (CuO) nanoparticles are prepared by the hydrothermal method which is used as a heterogeneous catalyst to synthesize 3-(2-chlorophenyl)-2,4-Pentadione. The energy band gap of HOMO-LUMO of CuO NPs is calculated using a UV-vis study which is found to be 1.96 eV. The crystalline development in the CuO NPs is investigated by X-ray peak broadening of the characteristic peak (111) of the XRD-diffractogram using Scherrer's formula, the average particle size (D), and d-spacing of the CuO NPs are evaluated 15.04 nm and 2.761 A°, respectively. The catalytic activity of CuO NPs is higher than the normal bulk form of CuO in the synthesis of3-(2-chlorophenyl)-2,4-Pentadione. The use of CuO NPs catalyst minimizes the reaction time. The percent yields of the product obtained by the same quantity and concentration of 5 mmol of CuO NPs and bulk CuO are 78 and 45, respectively. [ABSTRACT FROM AUTHOR] |
| Databáze: |
Complementary Index |
| Externí odkaz: |
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