Non-Destructive Evaluation of the AISI 304 Stainless Steel Susceptibility to Intergranular Corrosion by Electrical Conductivity Measurements.

Autor: Radojković, Bojana M., Jegdić, Bore V., Marunkić, Dunja D., Pejić, Jovanka N., Simović, Anđela R., Ćosović, Vladan R., Bajat, Jelena B.
Zdroj: Metals & Materials International; Mar2024, Vol. 30 Issue 3, p682-696, 15p
Abstrakt: This paper examined the degree of sensitization (DOS) to intergranular corrosion (IGC) and the level of electrical conductivity of the welded and non-welded AISI 304 stainless steel to obtain a suitable correlation. The DOS was determined by the double loop electrochemical potentiokinetic reactivation method (DL EPR), while the level of electrical conductivity was measured using a commercial device (non-destructive method). After electrochemical etching in oxalic acid, the microstructure of the specimen surface was analyzed by scanning electron microscopy (SEM). At DOS greater than ~ 0.5%, a clear linear dependence between the electrical conductivity and the value of the DOS was obtained, while there was a higher deviation from linearity for lower DOS values. The mentioned correlations were discussed in the sense of the precipitation kinetics of the Cr-carbide and the formation of Cr-depleted areas of different levels near the grain boundaries. Cr-depleted areas during anodic polarization measurements show lower resistance to pit formation. The presence of Cr-depleted areas in the vicinity of grain boundaries and the reduction of carbon content in the austenite crystal lattice increases the electrical conductivity of the stainless steel. [ABSTRACT FROM AUTHOR]
Databáze: Complementary Index