Eco-friendly Synthesis and Characterization of Amorphous Nanosilica from Rice Husk.

Autor: Pradeepkumar, S., Yassin, M. Mohamed, Marimuthu, S., Kalarani, M. K., Thiyageshwari, S., Gurumeenakshi, G.
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Zdroj: Agricultural Science Digest; Dec2023, Vol. 43 Issue 6, p790-795, 6p
Abstrakt: Background: A significant amount of rice production waste is rice husk. It is not humifiable and turns into a significant environmental pollutant if not properly utilized. Rice husk contains silica nanoparticles, which is a major inorganic component. High purity amorphous silica nanoparticles can thus be produced using simple thermo-chemical procedures without polluting the environment by cutting out the release of carbon dioxide during the process. Methods: A study was carried out to extract amorphous silica nanoparticles from rice husk ash using an environmentally benign chemical process. Utilising a variety of material characterization techniques viz., X-ray diffraction (XRD), fourier-transform infrared spectroscopy (FT-IR), field emission scanning electron microscope (FESEM), energy dispersive X-ray spectroscopy (EDS) and Particle size analyser (PSA), the extracted nanoparticles properties were confirmed. Result: The amorphous behaviour of the silica sample was confirmed using transmission electron microscopy-selected area electron diffraction patterns and X-ray diffraction analyses, whilst siloxane and silanol groups were primarily discovered using Fouriertransform infrared spectroscopy. Images obtained using scanning electron and transmission electron microscopy showed initial nanoparticles to be present along with secondary microparticles, possibly as a result of their agglomeration. The extracted amorphous silica has particles with an average diameter of 35 nm. This synthesized silica nanoparticles can be used in agriculture, nanoadditives, microelectronics, sensors and in other fields. [ABSTRACT FROM AUTHOR]
Databáze: Complementary Index