Preparation of a dicarbamate derivative and the development of cloud point extraction to determine the trace metals in water.

Autor: Al-Rekaby, Huda Turki, Mohammed, Imad J., Alkhikany, Abd-Al-Baqer
Předmět:
Zdroj: AIP Conference Proceedings; 2023, Vol. 2845 Issue 1, p1-14, 14p
Abstrakt: First step new reagents prepared. The reagents were diagnosed in the prepared through several known techniques such as NMRR, FT-IR, CHNS and Mass. Also, the study was complexes of the prepared reagent. A set of metals has been used by the studied optimal conditions were studied. In the follow step a cloud end confinement modus operandi was presented for the pre-concentration of down a bear ion in various samples. Investigate complexity by Hexyl carbamodithioate analyte ion are quantitatively extracted in (TritonX-114) following centrifugation. 1.0 mol/ L HCl nitric sharp in CH3OH was additional to the (surfactant-rich) steady old-fashioned previous to its analysis by (FAAS). (Triton X-114) and HCl and centrifuge rate, definite temperature and time were optimized. Recognition court for touch on ion was 0.091 ngmL−1. Limit of quantity (LOQ) (0.305 ng/ml), sensitivity (2×1−4) under optimum experimental conditions. The approach advanced has been successfully carried out to the determination of lead ion trace stages in electric energy plant water samples. [ABSTRACT FROM AUTHOR]
Databáze: Complementary Index