| Autor: |
Li, Longfei, Chen, Wanjiao, Xu, Zhongyun, Jiang, Jie, Zhang, Yong-Qiang |
| Předmět: |
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| Zdroj: |
Synthesis; Jul2023, Vol. 55 Issue 13, p2005-2010, 6p |
| Abstrakt: |
HRMS (ESI): I m i / I z i [M + H] SP + sp calcd for C SB 16 sb H SB 17 sb Br SB 2 sb O SB 2 sb : 398.9590; found: 398.9599. HRMS (ESI): I m i / I z i [M + H] SP + sp calcd for C SB 30 sb H SB 31 sb NO SB 2 sb S SB 2 sb : 502.1869; found: 502.1872. Naphthalen-1-yl 2-(3-(Benzyloxy)propyl)oxirane-2-carboxylate (8) Compound B 15 b (4.1 g, 15 mmol) was dissolved in a mixed solution of CF SB 3 sb CO SB 2 sb H (15 mL) and CH SB 2 sb Cl SB 2 sb (30 mL). Then the crude product was dissolved in dry CH SB 2 sb Cl SB 2 sb (30 mL) at 0 °C, Ph SB 3 sb P (1.8 g, 7 mmol) and CBr SB 4 sb (2.3 g, 7 mmol) were then added. [Extracted from the article] |
| Databáze: |
Complementary Index |
| Externí odkaz: |
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