Ultrasound-Assisted and One-Pot Synthesis of New Fe3O4/Mo-MOF Magnetic Nano Polymer as a Strong Antimicrobial Agent and Efficient Nanocatalyst in the Multicomponent Synthesis of Novel Pyrano[2,3-d]pyrimidines Derivatives.

Autor: Abdtawfeeq, Tarik Hafdhi, Farhan, Zainab A., Al-Majdi, Kadhum, Jawad, Mohammed Abed, Zabibah, Rahman S., Riadi, Yassine, Hadrawi, Salema K., AL-Alwany, Ameen, Shams, Marwah A.
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Zdroj: Journal of Inorganic & Organometallic Polymers & Materials; Feb2023, Vol. 33 Issue 2, p472-483, 12p
Abstrakt: A new Fe3O4/Mo-MOF (metal–organic framework) magnetic nano polymer was synthesized in one step and Ultrasound assisted. Fe3O4/Mo-MOF magnetic nano polymer was characterized by XRD, SEM, EDX mapping BET, VSM, and FT-IR. The results of the structure confirmation revealed that the ultrasonic method had created unique properties in the Fe3O4/Mo-MOF magnetic nano polymer, and its biological and catalytic applications were investigated. A new pyrano[2,3-d]pyrimidines derivative was synthesized using the catalytic activity of Fe3O4/Mo-MOF magnetic nano polymer in a three-component reaction involving malononitrile, aldehyde derivatives, and barbituric acid derivatives with Fe3O4/Mo-MOF magnetic nano polymer as a magnetic catalyst. In the antimicrobial activity of Fe3O4/Mo-MOF magnetic nano polymer: Antimicrobial properties on gram-positive, gram-negative, and fungal strains based on MIC, MBC, and MFC value. The results of catalytic and biological studies proved that nanoparticles have unique properties attributed to their structure and synthesis method. [ABSTRACT FROM AUTHOR]
Databáze: Complementary Index
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