High-pressure synthesis of borate-nitrates: crystal structure of M3B7O13(NO3) (M = Co2+, Ni2+, Cu2+, Zn2+, Cd2+).

Autor:	Pasqualini, Leonard C., Huppertz, Hubert
Předmět:	CRYSTAL structure SPACE groups CADMIUM compounds X-ray diffraction TRANSITION metals
Zdroj:	Zeitschrift für Naturforschung B: A Journal of Chemical Sciences; Oct2022, Vol. 77 Issue 10, p719-725, 7p
Abstrakt:	The orthorhombic nitrate-boracites with the sum formula M3B7O13NO3 (M = Co2+, Ni2+, Cu2+, Zn2+, Cd2+) were synthesized in a Walker-type multianvil apparatus under high-pressure/high-temperature conditions of 6 GPa and 800 °C, respectively. The crystal structures of the five isotypic substances, which crystallize in the space group Pca21, were determined via single-crystal X-ray diffraction and the structural features of the incorporated nitrate anions are discussed. [ABSTRACT FROM AUTHOR]
Databáze:	Complementary Index
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