| Autor: |
Kansiz, Sevgi, Agar, Tuggan, Dege, Necmi, Dogan, Onur Erman, Ahmede, Ruby, Saif, Eiad |
| Předmět: |
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| Zdroj: |
Acta Crystallographica Section E: Crystallographic Communications; Oct2020, Vol. 76 Issue 10, p1595-sup-4, 8p |
| Abstrakt: |
The title compound, C14H12INO, was synthesized by condensation of 2-hydroxy- 3-methylbenzaldehyde and 2-iodoaniline, and crystallizes in the orthorhombic space group P212121. The 2-iodophenyl and benzene rings are twisted with respect to each other, making a dihedral angle of 31.38 (2). The molecular structure is stabilized by an O--H N hydrogen bond, forming an S(6) ring motif. In the crystal, molecules are linked by O--H N interactions, resulting in the formation of sheets along the a-axis direction. Within the sheets, very weak stacking interactions lead to additional stabilization. The Hirshfeld surface analysis and fingerprint plots reveal that the crystal structure is dominated by H H (37.1%) and O--H N (30.1%) contacts. Hydrogen bonding and van der Waals interactions are the dominant interactions in the crystal packing. The crystal studied was refined as a two-component inversion twin. [ABSTRACT FROM AUTHOR] |
| Databáze: |
Complementary Index |
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