Synthesis of Pd-Fe System Alloy Nanoparticles by Pulsed Plasma in Liquid.

Autor: Tamura, Shota, Mashimo, Tsutomu, Yamamoto, Kenta, Kelgenbaeva, Zhazgul, Ma, Weijan, Kang, Xuesong, Koinuma, Michio, Isobe, Hiroshi, Yoshiasa, Akira
Předmět:
Zdroj: Nanomaterials (2079-4991); Dec2018, Vol. 8 Issue 12, p1068, 1p
Abstrakt: We synthesized Pd-Fe series nanoparticles in solid solution using pulsed plasma in liquid with Pd-Fe bulk mixture electrodes. The Pd-Fe atomic percent ratios were 1:3, 1:1, and 3:1, and the particle size was measured to be less than 10 nm by high-resolution transmission electron microscopy (HR-TEM). The nanoparticles showed face-centered cubic structure. The lattice parameter increased with increasing Pd content and followed Vegard's law, and energy-dispersive X-ray spectra were consistent with the ratios of the starting samples, which showed a solid solution state. The solid solution structure and local structure were confirmed by HR-TEM and X-ray absorption fine structure. [ABSTRACT FROM AUTHOR]
Databáze: Complementary Index