Synthesis, Characterization, Crystal Structure, and Hirshfeld Surface Analysis of Ethyl 2-(4-bromophenyl)-1-cyclohexyl-1H-benzo[d]imidazole-5-carboxylate.

Autor: Nikil, P., Poojary, Boja, Kumar, S. Madan, Byrappa, K.
Předmět:
Zdroj: Crystallography Reports; Jul2018, Vol. 63 Issue 4, p574-580, 7p
Abstrakt: The title compound, C22H23N2BrO2 was synthesized via one-pot reductive cyclization method and characterized by CNH analysis, FT-IR, UV-visible, mass, 1H and 13C NMR spectra, thermogravimetric analysis (TGA) and single crystal X-ray diffraction method. The compound crystallizes in monoclinic crystal system: sp. gr. P21/c, Z = 4. The crystal data reveals that the intermolecular interactions of the C-H···π and π···π type connect the molecules which was also visualized with the help of Hirshfeld surface analysis. [ABSTRACT FROM AUTHOR]
Databáze: Complementary Index