A Convenient One‐Pot Synthesis of Thieno[2′,3′:4,5]Pyrimido[1,2‐b]‐[1,2,4,5]Tetrazines.

Autor: Hassan, Allam A., Khattab, Reham R., Wasfy, Ashraf A. F., Abuzeid, Khadiga M., Hassan, Nasser A.
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Zdroj: Journal of Heterocyclic Chemistry; Apr2018, Vol. 55 Issue 4, p907-912, 6p
Abstrakt: A novel series of thieno[2′,3′:4,5]pyrimido[1,2‐b][1,2,4,5]tetrazin‐6‐one derivatives 14 were prepared from the reaction of 3‐amino‐2‐thioxo‐1,2,3,5,6,7‐hexahydro‐4H‐cyclopenta[4,5]thieno[2,3‐d]pyrimidin‐4‐one 3 or its methylthio 4 with hydrazonoyl chlorides 9. The mechanism of the studied reactions has been discussed and further evidence for the assigned structure of the products is based on alternative synthesis. A single crystal X‐ray analysis of compound 14e has been carried out. [ABSTRACT FROM AUTHOR]
Databáze: Complementary Index
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