Autor: |
Yantao Chen, Aurell, Carl-Johan, Korsgren, Pernilla, Malm, Johanna, Härslätt, Malin, Fridén-Saxin, Maria, Pettersen, Anna |
Předmět: |
|
Zdroj: |
Synthesis; 2018, Vol. 50 Issue 7, p1471-1481, 11p |
Abstrakt: |
A key intermediate was obtained as solid through filtration of the reaction mixture of saccharin, chloro(triphenyl)phosphonium chloride, and N,N-diisopropylethylamine (DIPEA) in chloroform. The soluble triphenylphosphine oxide went to filtrate as waste, while the solid was reacted with amines to afford N-sulfonylamidines. In total, 26 N-sulfonylamidine products were obtained in moderate to good overall yields. [ABSTRACT FROM AUTHOR] |
Databáze: |
Complementary Index |
Externí odkaz: |
|