Autor: |
Al-Rubaye, Baidaa K., Brink, Alice, Miller, Gary J., Potgieter, Herman, Al-Jeboori, Mohamad J. |
Předmět: |
|
Zdroj: |
Acta Crystallographica Section E: Crystallographic Communications; Jul2017, Vol. 73 Issue 7, p1092-1096, 16p |
Abstrakt: |
The preparation of the title compound, C26H25N, was achieved by the condensation of an ethanolic mixture of benzaldehyde, cyclohexanone and ammonium acetate in a 2:1:1 molar ratio. There are two crystallographically independent molecules in the asymmetric unit. The two cyclohexyl rings adopt an anti-envelope conformation with the benzyl moiety adopting a cis conformation with respect to the nitrogen atom of the phenanthridine segment. In the crystal, molecules are linked through C-H⋯N interactions into hydrogen-bonded chains that are further arranged into distinct layers by weak offset π-π interactions. [ABSTRACT FROM AUTHOR] |
Databáze: |
Complementary Index |
Externí odkaz: |
|