Polysilicic Acid Gel Method Derived V2O5/Sio2 Composite Materials: Synthesis and Characterization.

Autor: Dawei Wang, Linzong Zhou, Xiaofei Feng, Ning Zhao, Bin Yang
Předmět:
Zdroj: AIP Conference Proceedings; 2017, Vol. 1794 Issue 1, p1-5, 5p, 1 Black and White Photograph, 2 Graphs
Abstrakt: The V2O5/SiO2 composite was prepared by a sol-gel method followed a sintering procedure. The low-cost Na2SiO39H2O was used as silicon source, while NH4VO3 was used as vanadium source. By adding NH4VO3 to Na2SiO3 solution and adjusting the mixture's pH with saturated (NH4)2SO4 solution the polysilicic acid gel was formed to give a homogeneous gel composite with VO3- well-distributed in it. The gel composite was dried at 100 °C to give the xerogel, then the xerogel was calcined in air to obtain the V2O5/SiO2 composite. The V2O5/SiO2 composites were characterized by SEM analysis, FT-IR spectroscopy and powder X-ray diffractions. [ABSTRACT FROM AUTHOR]
Databáze: Complementary Index