| Autor: |
Dighore, Nitin R., Anandgaonker, Priyanka L., Gaikwad, Suresh T., Rajbhoj, Anjali S. |
| Předmět: |
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| Zdroj: |
Materials Science-Poland; Mar2015, Vol. 33 Issue 1, p163-168, 6p |
| Abstrakt: |
Crystalline MoO3 nanoparticles were obtained by electrochemical synthesis process using tetrapropylammonium bromide as a stabilizer and structure-directing agent in ACN:THF(4:1) solvent. Formation of MoO3 nanoparticles took place at a constant supply current of 14 mA/cm2. These synthesized MoO3 nanoparticles were characterized by UV-Vis spectroscopy, FT-IR spectroscopy, powder X-ray diffraction (XRD), scanning electron microscopy (SEM). So prepared MoO3 nanoparticles were used as a heterogeneous catalyst for the synthesis of 2,6-bis(benzylidene)cyclohexanone derivatives. This protocol offers several advantages, such as simple work-up procedure, recyclability of the catalyst, excellent product yield in a short reaction time and purification of products with a non-chromatographic method. [ABSTRACT FROM AUTHOR] |
| Databáze: |
Complementary Index |
| Externí odkaz: |
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