Catalyst-Free Synthesis of Spiropyrazolines from Chalcones and Cyclic Ketone N-Tosylhydrazones.

Autor: Qin-Xi Wu, Hui-Jing Li, Hong-Shuang Wang, Zhen-Guo Zhang, Chen-Chao Wang, Yan-Chao Wu
Předmět:
Zdroj: Synlett; 2015, Vol. 26 Issue 2, p243-249, 7p
Abstrakt: Treatment of cyclic ketone N-tosylhydrazones with chalcones in the presence of cesium carbonate at 110 °C affords spiropyrazolines with high selectivity and excellent yields. This protocol possesses many advantages such as readily available and stable starting materials, high selectivity, operational simplicity, and catalyst-free conditions. [ABSTRACT FROM AUTHOR]
Databáze: Complementary Index