A green and efficient approach for the simultaneous extraction and mechanisms of essential oil and lignin from Cinnamomum camphora: Process optimization based on deep learning.

Autor: Yang H; College of Materials Science and Engineering, Central South University of Forestry and Technology, Changsha 410004, Hunan, China., Zhou P; College of Materials Science and Engineering, Central South University of Forestry and Technology, Changsha 410004, Hunan, China., Li X; College of Materials Science and Engineering, Central South University of Forestry and Technology, Changsha 410004, Hunan, China; Institute of Natural Products Research and Development, Central South University of Forestry and Technology, Changsha 410004, Hunan, China. Electronic address: rlxz@163.com., Shen L; Key Laboratory of Chemistry and Engineering of Forest Products, State Ethnic Affairs Commission, Guangxi Key Laboratory of Chemistry and Engineering of Forest Products, Guangxi Collaborative Innovation Center for Chemistry and Engineering of Forest Products, Guangxi Minzu University, Nanning 530006, Guangxi, China.
Jazyk: angličtina
Zdroj: International journal of biological macromolecules [Int J Biol Macromol] 2024 Oct; Vol. 277 (Pt 4), pp. 134215. Date of Electronic Publication: 2024 Jul 27.
DOI: 10.1016/j.ijbiomac.2024.134215
Abstrakt: The utilization and economic benefits of biomass resources can be maximized through rational design and process optimization. In this study, an innovative approach for the simultaneous extraction of essential oil and lignin from Cinnamomum camphora leaves by deep eutectic solvent (DES) and optimization of the process parameters was achieved using deep learning tools. With the water content of 40 %, liquid-solid ratio of 9.00 mL/g, and distillation time of 51.81 min, the yields of the essential oil and lignin reached 3.15 ± 0.02 % and 9.75 ± 0.15 %, respectively. Notably, the efficiency of simultaneous extraction of essential oil improved by 23 % compared to that of traditional steam distillation. Moreover, the extraction mechanism of the process was clarified. The connection between lignin with cellulose and hemicellulose was disintegrated by the DES, resulting in lignin shedding and hence accelerating the dissolution of essential oil. Moreover, the compositions of lignin and essential oil were also identified.
Competing Interests: Declaration of competing interest We declare that we do not have any commercial or associative interest that represents a conflict of interest in connection with the work submitted.
(Copyright © 2024. Published by Elsevier B.V.)
Databáze: MEDLINE