Exploring the Impact of Different Milling Parameters of Fe/SiO 2 Composites on Their Structural and Magnetic Properties.

Autor: Rudeichuk T; Institute of Manufacturing Management, Faculty of Manufacturing Technologies, Technical University of Košice, Bayerova 1, 08001 Prešov, Slovakia., Olekšáková D; Institute of Manufacturing Management, Faculty of Manufacturing Technologies, Technical University of Košice, Bayerova 1, 08001 Prešov, Slovakia., Maciaszek R; Institute of Physics, Faculty of Science, Pavol Jozef Šafárik University in Košice, Park Angelinum 9, 04154 Košice, Slovakia., Matysiak W; Institute of Materials Technology, Faculty of Mechanical Engineering, Poznan University of Technology, Piotrowo 3, 60-965 Poznan, Poland., Kollár P; Institute of Physics, Faculty of Science, Pavol Jozef Šafárik University in Košice, Park Angelinum 9, 04154 Košice, Slovakia.
Jazyk: angličtina
Zdroj: Materials (Basel, Switzerland) [Materials (Basel)] 2024 Feb 12; Vol. 17 (4). Date of Electronic Publication: 2024 Feb 12.
DOI: 10.3390/ma17040862
Abstrakt: This research focuses on the production process of soft magnetic composites in the form of 3D bulk compacts made from insulated powder particles using different milling parameters, aiming to enhance their magnetic properties and to study an innovative method of the powder surface "smoothing" technique. A structure analysis using scanning electron microscopy (SEM), EDS, and optical microscopy is also included. We found out that the samples made by the innovative method have lower density values. This can be caused by a more consistent SiO 2 insulation layer on highly pure iron powder particles. A correlation between the mechanical smoothing method and better insulation of powder particles can help to provide eco-friendlier solutions for the preparation of soft magnetic composites, such as less usage of reagents and more consistent coverage of powder particles with lower final insulation thickness. The magnetic properties of these compacts are evaluated by coercive field, permeability, and loss measurements. The particle-level smoothing technique in some cases can reduce the value of coercivity up to 20%. For some samples, the ball-to-powder ratio has a bigger impact on magnetic properties than surface treatment, which can be caused by an increased amount of insulation in the SMC compacts.
Databáze: MEDLINE
Nepřihlášeným uživatelům se plný text nezobrazuje