CAT on MOUSE: Control and automation of temperature for single-sided NMR instruments such as NMR-MOUSE.

Autor: Mailhiot S; NMR Research Unit, University of Oulu, Oulu, Finland., Mankinen O; NMR Research Unit, University of Oulu, Oulu, Finland., Li J; NMR Research Unit, University of Oulu, Oulu, Finland.; NIMBE, CEA, CNRS, Université de Paris Saclay, CEA Saclay, Gif-sur-Yvette, France., Kharbanda Y; NMR Research Unit, University of Oulu, Oulu, Finland.; Laboratoire Navier (Ecole des Ponts ParisTech-Université Gustave Eiffel), Champs-sur-Marne, France., Telkki VV; NMR Research Unit, University of Oulu, Oulu, Finland., Urbańczyk M; Institute of Physical Chemistry, Polish Academy of Sciences, Warsaw, Poland.
Jazyk: angličtina
Zdroj: Magnetic resonance in chemistry : MRC [Magn Reson Chem] 2024 Apr; Vol. 62 (4), pp. 252-258. Date of Electronic Publication: 2023 Jun 21.
DOI: 10.1002/mrc.5376
Abstrakt: Temperature-dependent experiments are a rapidly growing area of interest for low-field NMR. In this work, we present a new device for wide-range temperature control for single-sided NMR instruments. The presented device, called CAT, is simple to build, inexpensive, and easy to modify to accommodate different samples. We present the capabilities of the device using a freezing temperature study of acetic acid/water mixtures. Additionally, we present the stability of the device over long measurement times. We believe that by introducing such a device with an open-source design, we allow researchers to use it in a wide range of applications and to fully incorporate variable-temperature studies in the world of single-sided instruments.
(© 2023 The Authors. Magnetic Resonance in Chemistry published by John Wiley & Sons Ltd.)
Databáze: MEDLINE
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