Multi-class, multi-residue determination of 132 veterinary drugs in milk by magnetic solid-phase extraction based on magnetic hypercrosslinked polystyrene prior to their determination by high-performance liquid chromatography-tandem mass spectrometry.
Autor: | Melekhin AO; Department of Chemistry, Lomonosov Moscow State University, Leninskie gory, 1/3, 119991 Moscow, Russia; Central Scientific Methodological Veterinary Laboratory, Orangereynaya st., 23, 111622 Moscow, Russia., Tolmacheva VV; Department of Chemistry, Lomonosov Moscow State University, Leninskie gory, 1/3, 119991 Moscow, Russia., Goncharov NO; Department of Chemistry, Lomonosov Moscow State University, Leninskie gory, 1/3, 119991 Moscow, Russia., Apyari VV; Department of Chemistry, Lomonosov Moscow State University, Leninskie gory, 1/3, 119991 Moscow, Russia. Electronic address: apyari@mail.ru., Dmitrienko SG; Department of Chemistry, Lomonosov Moscow State University, Leninskie gory, 1/3, 119991 Moscow, Russia., Shubina EG; Central Scientific Methodological Veterinary Laboratory, Orangereynaya st., 23, 111622 Moscow, Russia., Grudev AI; Central Scientific Methodological Veterinary Laboratory, Orangereynaya st., 23, 111622 Moscow, Russia. |
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Jazyk: | angličtina |
Zdroj: | Food chemistry [Food Chem] 2022 Sep 01; Vol. 387, pp. 132866. Date of Electronic Publication: 2022 Mar 31. |
DOI: | 10.1016/j.foodchem.2022.132866 |
Abstrakt: | A quantitative multi-class multi-residue analytical method was developed for the determination of veterinary drugs in milk by high-performance liquid chromatography - tandem mass spectrometry (HPLC-MS/MS). A total of 132 veterinary drugs investigated belonged to almost 15 classes including sulfonamides, β-lactams, tetracyclines, quinolones, macrolides, nitrofurans, nitroimidazoles, phenicols, lincosamides, pleuromutilins, macrocyclic lactones, quinoxaline antibiotics, benzimidazoles, anthelmintics, coccidiostats and some others. A magnetic solid-phase extraction procedure was developed using magnetic hypercrosslinked polystyrene (HCP/Fe (Copyright © 2022 Elsevier Ltd. All rights reserved.) |
Databáze: | MEDLINE |
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