Versailles project on advanced materials and standards (VAMAS) interlaboratory study on measuring the number concentration of colloidal gold nanoparticles.

Autor: Minelli C; Chemical & Biological Sciences Department, National Physical Laboratory, Hampton Road, Teddington TW11 0LW, UK. caterina.minelli@npl.co.uk., Wywijas M; Chemical & Biological Sciences Department, National Physical Laboratory, Hampton Road, Teddington TW11 0LW, UK. caterina.minelli@npl.co.uk., Bartczak D; National Measurement Laboratory, Queens road, Teddington TW11 0LY, UK., Cuello-Nuñez S; National Measurement Laboratory, Queens road, Teddington TW11 0LY, UK., Infante HG; National Measurement Laboratory, Queens road, Teddington TW11 0LY, UK., Deumer J; Physikalisch-Technische Bundesanstalt (PTB), Abbestr. 2-12, 10587 Berlin, Germany., Gollwitzer C; Physikalisch-Technische Bundesanstalt (PTB), Abbestr. 2-12, 10587 Berlin, Germany., Krumrey M; Physikalisch-Technische Bundesanstalt (PTB), Abbestr. 2-12, 10587 Berlin, Germany., Murphy KE; National Institute of Standards and Technology, 100 Bureau Drive, Gaithersburg, Maryland 20899-8391, USA., Johnson ME; National Institute of Standards and Technology, 100 Bureau Drive, Gaithersburg, Maryland 20899-8391, USA., Montoro Bustos AR; National Institute of Standards and Technology, 100 Bureau Drive, Gaithersburg, Maryland 20899-8391, USA., Strenge IH; National Institute of Standards and Technology, 100 Bureau Drive, Gaithersburg, Maryland 20899-8391, USA., Faure B; Xenocs SAS, 1-3 Allée du Nanomètre, 38000 Grenoble, France., Høghøj P; Xenocs SAS, 1-3 Allée du Nanomètre, 38000 Grenoble, France., Tong V; Chemical & Biological Sciences Department, National Physical Laboratory, Hampton Road, Teddington TW11 0LW, UK. caterina.minelli@npl.co.uk., Burr L; CSEM SA, Bahnhofstrasse 1, 7242 Landquart, Switzerland., Norling K; Chalmers University of Technology, Gothenburg 412 96, Sweden., Höök F; Chalmers University of Technology, Gothenburg 412 96, Sweden., Roesslein M; Empa, Swiss Federal Laboratories for Material Science and Technology, Lerchenfeldstrasse 5, CH-9014 St Gallen, Switzerland., Kocic J; ETH Zurich, Vladimir-Prelog-Weg 1, 8093 Zurich, Switzerland., Hendriks L; ETH Zurich, Vladimir-Prelog-Weg 1, 8093 Zurich, Switzerland., Kestens V; European Commission, Joint Research Centre (JRC), Geel, Belgium., Ramaye Y; European Commission, Joint Research Centre (JRC), Geel, Belgium., Contreras Lopez MC; European Commission, Joint Research Centre (JRC), Geel, Belgium., Auclair G; European Commission, Joint Research Centre (JRC), Geel, Belgium., Mehn D; European Commission, Joint Research Centre (JRC), Ispra, Italy., Gilliland D; European Commission, Joint Research Centre (JRC), Ispra, Italy., Potthoff A; Fraunhofer Institute for Ceramic Technologies and Systems IKTS, Winterbergstr. 28, 01217 Dresden, Germany., Oelschlägel K; Fraunhofer Institute for Ceramic Technologies and Systems IKTS, Winterbergstr. 28, 01217 Dresden, Germany., Tentschert J; The German Federal Institute for Risk Assessment, Max-Dohrn Str. 8-10, Berlin, Germany., Jungnickel H; The German Federal Institute for Risk Assessment, Max-Dohrn Str. 8-10, Berlin, Germany., Krause BC; The German Federal Institute for Risk Assessment, Max-Dohrn Str. 8-10, Berlin, Germany., Hachenberger YU; The German Federal Institute for Risk Assessment, Max-Dohrn Str. 8-10, Berlin, Germany., Reichardt P; The German Federal Institute for Risk Assessment, Max-Dohrn Str. 8-10, Berlin, Germany., Luch A; The German Federal Institute for Risk Assessment, Max-Dohrn Str. 8-10, Berlin, Germany., Whittaker TE; Department of Materials, Department of Bioengineering and Institute of Biomedical Engineering, Imperial College London, Exhibition road, London SW7 2BX, UK., Stevens MM; Department of Materials, Department of Bioengineering and Institute of Biomedical Engineering, Imperial College London, Exhibition road, London SW7 2BX, UK., Gupta S; Indian Institute of Technology Delhi, New Delhi 110016, India., Singh A; Indian Institute of Technology Delhi, New Delhi 110016, India., Lin FH; Centre for Measurement Standards, Industrial Technology Research Institute, No. 321, Sec. 2, Kuang Fu Rd., Hsinchu, 30011, Taiwan, Republic of China., Liu YH; Centre for Measurement Standards, Industrial Technology Research Institute, No. 321, Sec. 2, Kuang Fu Rd., Hsinchu, 30011, Taiwan, Republic of China., Costa AL; Institute of Science and Technology for Ceramics, Via Granarolo 64, 48018 Faenza, Italy., Baldisserri C; Institute of Science and Technology for Ceramics, Via Granarolo 64, 48018 Faenza, Italy., Jawad R; Karolinska Institutet, 171 77 Stockholm, Sweden., Andaloussi SEL; Karolinska Institutet, 171 77 Stockholm, Sweden., Holme MN; Karolinska Institutet, 171 77 Stockholm, Sweden.; Department of Materials, Department of Bioengineering and Institute of Biomedical Engineering, Imperial College London, Exhibition road, London SW7 2BX, UK., Lee TG; Korea Research Institute of Standards and Science (KRISS), 267 Gajeong-ro, Yuseong-gu, Daejeon 34113, Korea., Kwak M; Korea Research Institute of Standards and Science (KRISS), 267 Gajeong-ro, Yuseong-gu, Daejeon 34113, Korea., Kim J; Korea Research Institute of Standards and Science (KRISS), 267 Gajeong-ro, Yuseong-gu, Daejeon 34113, Korea., Ziebel J; Luxembourg Institute of Science and Technology, 41 rue du Brill, L-4422 Belvaux, Luxembourg., Guignard C; Luxembourg Institute of Science and Technology, 41 rue du Brill, L-4422 Belvaux, Luxembourg., Cambier S; Luxembourg Institute of Science and Technology, 41 rue du Brill, L-4422 Belvaux, Luxembourg., Contal S; Luxembourg Institute of Science and Technology, 41 rue du Brill, L-4422 Belvaux, Luxembourg., Gutleb AC; Luxembourg Institute of Science and Technology, 41 rue du Brill, L-4422 Belvaux, Luxembourg., Kuba Tatarkiewicz J; MANTA Instruments, Inc., San Diego, CA, USA., Jankiewicz BJ; Military University of Technology, gen. Sylwestra Kaliskiego 2 str., 00-908 Warsaw, Poland., Bartosewicz B; Military University of Technology, gen. Sylwestra Kaliskiego 2 str., 00-908 Warsaw, Poland., Wu X; National Center for Nanoscience and Technology (NCNST), No. 11, ZhongGuanCun BeiYiTiao, Beijing 100190, People's Republic of China., Fagan JA; National Institute of Standards and Technology, 100 Bureau Drive, Gaithersburg, Maryland 20899-8391, USA., Elje E; NILU-Norwegian Institute for Air Research, Instituttveien 18, 2007 Kjeller, Norway.; University of Oslo, Sognsvannsveien 9, 0372 Oslo, Norway., Rundén-Pran E; NILU-Norwegian Institute for Air Research, Instituttveien 18, 2007 Kjeller, Norway., Dusinska M; NILU-Norwegian Institute for Air Research, Instituttveien 18, 2007 Kjeller, Norway., Kaur IP; Nottingham Trent University, 50 Shakespeare St, Nottingham NG1 4FQ, UK., Price D; PerkinElmer, Chalfont Road, Seer Green, Bucks HP92FX, UK., Nesbitt I; Public Analyst's Laboratory, Sir Patrick Duns, Lower Grand Canal Street, Dublin 2, D02 P667, Ireland., O Reilly S; Public Analyst's Laboratory, Sir Patrick Duns, Lower Grand Canal Street, Dublin 2, D02 P667, Ireland., Peters RJB; Wageningen Food Safety Research, Wageningen University & Research, Akkermaalsbos 2, 6708 WB Wageningen, The Netherlands., Bucher G; Service Commun des Laboratoires, 3 Avenue Dr Albert Schweitzer, 33600 Pessac, France., Coleman D; Smith+Nephew, 101 Hessle Road, Hull HU3 2BN, UK., Harrison AJ; Smith+Nephew, 101 Hessle Road, Hull HU3 2BN, UK., Ghanem A; SOLVAY Research & Innovation, Brussels Centre, Rue de Ransbeek 310, 1120 Brussels, Belgium., Gering A; SOLVAY Research & Innovation, Brussels Centre, Rue de Ransbeek 310, 1120 Brussels, Belgium., McCarron E; State Laboratory, Backweston Campus, Young's Cross, Celbridge, Co Kildare, W23 VW2C, Ireland., Fitzgerald N; State Laboratory, Backweston Campus, Young's Cross, Celbridge, Co Kildare, W23 VW2C, Ireland., Cornelis G; Swedish University of Agricultural Sciences, Lennart Hjelms väg 9, 75651 Uppsala, Sweden., Tuoriniemi J; Swedish University of Agricultural Sciences, Lennart Hjelms väg 9, 75651 Uppsala, Sweden., Sakai M; Toray Research Center, Inc., 3-3-7 Sonoyama, Otsu, Shiga 5208567, Japan., Tsuchida H; Toray Research Center, Inc., 3-3-7 Sonoyama, Otsu, Shiga 5208567, Japan., Maguire C; Trinity Translational Medicine Institute, Trinity College Dublin, Dublin, Ireland., Prina-Mello A; Trinity Translational Medicine Institute, Trinity College Dublin, Dublin, Ireland., Lawlor AJ; UK centre for Ecology and Hydrology, Lancaster Environment Centre, Library Avenue, Bailrigg, Lancaster LA1 4AP, UK., Adams J; UK centre for Ecology and Hydrology, Lancaster Environment Centre, Library Avenue, Bailrigg, Lancaster LA1 4AP, UK., Schultz CL; UK Centre for Ecology and Hydrology, Maclean Building, Benson Lane, Crowmarsh-Gifford, Wallingford, OX10 8BB, UK., Constantin D; Laboratoire de Physique des Solides, Université Paris-Saclay, CNRS, 91405 Orsay, France., Thanh NTK; Department of Physics and Astronomy, University College London, Gower Street, London WC1E 6BT, UK., Tung LD; Department of Physics and Astronomy, University College London, Gower Street, London WC1E 6BT, UK., Panariello L; Department of Chemical Engineering, University College London, Torrington Place, London, WC1E 7JE, UK., Damilos S; Department of Chemical Engineering, University College London, Torrington Place, London, WC1E 7JE, UK., Gavriilidis A; Department of Chemical Engineering, University College London, Torrington Place, London, WC1E 7JE, UK., Lynch I; School of Geography, Earth and Environmental Sciences, University of Birmingham, Edgbaston, B15 2TT Birmingham, UK., Fryer B; School of Geography, Earth and Environmental Sciences, University of Birmingham, Edgbaston, B15 2TT Birmingham, UK., Carrazco Quevedo A; School of Geography, Earth and Environmental Sciences, University of Birmingham, Edgbaston, B15 2TT Birmingham, UK., Guggenheim E; School of Geography, Earth and Environmental Sciences, University of Birmingham, Edgbaston, B15 2TT Birmingham, UK., Briffa S; School of Geography, Earth and Environmental Sciences, University of Birmingham, Edgbaston, B15 2TT Birmingham, UK., Valsami-Jones E; School of Geography, Earth and Environmental Sciences, University of Birmingham, Edgbaston, B15 2TT Birmingham, UK., Huang Y; Bren School of Environmental Science and Management, University of California at Santa Barbara, CA, 93106, USA., Keller AA; Bren School of Environmental Science and Management, University of California at Santa Barbara, CA, 93106, USA., Kinnunen VT; Department of Chemistry, University of Jyväskylä, P.O. Box 35, FI-40014 Jyväskylä, Finland., Perämäki S; Department of Chemistry, University of Jyväskylä, P.O. Box 35, FI-40014 Jyväskylä, Finland., Krpetic Z; School of Science Engineering and Environment, University of Salford, M5 4WT Salford, UK., Greenwood M; School of Science Engineering and Environment, University of Salford, M5 4WT Salford, UK., Shard AG; Chemical & Biological Sciences Department, National Physical Laboratory, Hampton Road, Teddington TW11 0LW, UK. caterina.minelli@npl.co.uk.
Jazyk: angličtina
Zdroj: Nanoscale [Nanoscale] 2022 Mar 24; Vol. 14 (12), pp. 4690-4704. Date of Electronic Publication: 2022 Mar 24.
DOI: 10.1039/d1nr07775a
Abstrakt: We describe the outcome of a large international interlaboratory study of the measurement of particle number concentration of colloidal nanoparticles, project 10 of the technical working area 34, "Nanoparticle Populations" of the Versailles Project on Advanced Materials and Standards (VAMAS). A total of 50 laboratories delivered results for the number concentration of 30 nm gold colloidal nanoparticles measured using particle tracking analysis (PTA), single particle inductively coupled plasma mass spectrometry (spICP-MS), ultraviolet-visible (UV-Vis) light spectroscopy, centrifugal liquid sedimentation (CLS) and small angle X-ray scattering (SAXS). The study provides quantitative data to evaluate the repeatability of these methods and their reproducibility in the measurement of number concentration of model nanoparticle systems following a common measurement protocol. We find that the population-averaging methods of SAXS, CLS and UV-Vis have high measurement repeatability and reproducibility, with between-labs variability of 2.6%, 11% and 1.4% respectively. However, results may be significantly biased for reasons including inaccurate material properties whose values are used to compute the number concentration. Particle-counting method results are less reproducibile than population-averaging methods, with measured between-labs variability of 68% and 46% for PTA and spICP-MS respectively. This study provides the stakeholder community with important comparative data to underpin measurement reproducibility and method validation for number concentration of nanoparticles.
Databáze: MEDLINE