| Autor: |
Kataev SS; Perm Regional Bureau of Forensic-Medical Expertise, Perm, Russia., Dvorskaya ON; Perm State Pharmaceutical Academy of the Ministry of Health, Perm, Russia., Gofenberg MA; Regional Narcological Hospital, Yekaterinburg, Russia.; Ural State Medical University of the Ministry of Health of Russia, Yekaterinburg, Russia. |
| Jazyk: |
ruština |
| Zdroj: |
Sudebno-meditsinskaia ekspertiza [Sud Med Ekspert] 2021; Vol. 64 (1), pp. 29-33. |
| DOI: |
10.17116/sudmed20216401129 |
| Abstrakt: |
The purpose of this work is to study the possibility of using cartridges with a mixed sorbent C8/SAX for the extraction of synthetic cannabimimetic metabolites MDMB (N)-073F from urine. It was used enzymatic hydrolysis of urine, solid phase extraction using cartridges C8/SAX and C8/SCX with mixed phase, derivatization and gas chromatography with a mass spectrometric detector. The results of the study allow us to recommend cartridges for solid-phase extraction with an anion-exchange phase (C8/SAX or SAX) when conducting a targeted study for the presence of cannabimimetics metabolites that have compounds with a carboxyl group as the main metabolites. |
| Databáze: |
MEDLINE |
| Externí odkaz: |
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