BioMAX - the first macromolecular crystallography beamline at MAX IV Laboratory.

Autor: Ursby T; MAX IV Laboratory, Lund University, PO Box 118, S-221 00 Lund, Sweden., Åhnberg K; MAX IV Laboratory, Lund University, PO Box 118, S-221 00 Lund, Sweden., Appio R; MAX IV Laboratory, Lund University, PO Box 118, S-221 00 Lund, Sweden., Aurelius O; MAX IV Laboratory, Lund University, PO Box 118, S-221 00 Lund, Sweden., Barczyk A; MAX IV Laboratory, Lund University, PO Box 118, S-221 00 Lund, Sweden., Bartalesi A; MAX IV Laboratory, Lund University, PO Box 118, S-221 00 Lund, Sweden., Bjelčić M; MAX IV Laboratory, Lund University, PO Box 118, S-221 00 Lund, Sweden., Bolmsten F; MAX IV Laboratory, Lund University, PO Box 118, S-221 00 Lund, Sweden., Cerenius Y; MAX IV Laboratory, Lund University, PO Box 118, S-221 00 Lund, Sweden., Doak RB; Department of Biomolecular Mechanisms, Max Planck Institute for Medical Research, Jahnstrasse 29, 69120 Heidelberg, Germany., Eguiraun M; MAX IV Laboratory, Lund University, PO Box 118, S-221 00 Lund, Sweden., Eriksson T; MAX IV Laboratory, Lund University, PO Box 118, S-221 00 Lund, Sweden., Friel RJ; MAX IV Laboratory, Lund University, PO Box 118, S-221 00 Lund, Sweden., Gorgisyan I; MAX IV Laboratory, Lund University, PO Box 118, S-221 00 Lund, Sweden., Gross A; MAX IV Laboratory, Lund University, PO Box 118, S-221 00 Lund, Sweden., Haghighat V; MAX IV Laboratory, Lund University, PO Box 118, S-221 00 Lund, Sweden., Hennies F; MAX IV Laboratory, Lund University, PO Box 118, S-221 00 Lund, Sweden., Jagudin E; MAX IV Laboratory, Lund University, PO Box 118, S-221 00 Lund, Sweden., Norsk Jensen B; MAX IV Laboratory, Lund University, PO Box 118, S-221 00 Lund, Sweden., Jeppsson T; MAX IV Laboratory, Lund University, PO Box 118, S-221 00 Lund, Sweden., Kloos M; Department of Biomolecular Mechanisms, Max Planck Institute for Medical Research, Jahnstrasse 29, 69120 Heidelberg, Germany., Lidon-Simon J; MAX IV Laboratory, Lund University, PO Box 118, S-221 00 Lund, Sweden., de Lima GMA; MAX IV Laboratory, Lund University, PO Box 118, S-221 00 Lund, Sweden., Lizatovic R; MAX IV Laboratory, Lund University, PO Box 118, S-221 00 Lund, Sweden., Lundin M; MAX IV Laboratory, Lund University, PO Box 118, S-221 00 Lund, Sweden., Milan-Otero A; MAX IV Laboratory, Lund University, PO Box 118, S-221 00 Lund, Sweden., Milas M; MAX IV Laboratory, Lund University, PO Box 118, S-221 00 Lund, Sweden., Nan J; MAX IV Laboratory, Lund University, PO Box 118, S-221 00 Lund, Sweden., Nardella A; MAX IV Laboratory, Lund University, PO Box 118, S-221 00 Lund, Sweden., Rosborg A; MAX IV Laboratory, Lund University, PO Box 118, S-221 00 Lund, Sweden., Shilova A; MAX IV Laboratory, Lund University, PO Box 118, S-221 00 Lund, Sweden., Shoeman RL; Department of Biomolecular Mechanisms, Max Planck Institute for Medical Research, Jahnstrasse 29, 69120 Heidelberg, Germany., Siewert F; Helmholtz Zentrum Berlin für Materialien und Energie, Albert-Einstein-Strasse 15, DE-12489 Berlin, Germany., Sondhauss P; MAX IV Laboratory, Lund University, PO Box 118, S-221 00 Lund, Sweden., Talibov VO; MAX IV Laboratory, Lund University, PO Box 118, S-221 00 Lund, Sweden., Tarawneh H; MAX IV Laboratory, Lund University, PO Box 118, S-221 00 Lund, Sweden., Thånell J; MAX IV Laboratory, Lund University, PO Box 118, S-221 00 Lund, Sweden., Thunnissen M; MAX IV Laboratory, Lund University, PO Box 118, S-221 00 Lund, Sweden., Unge J; MAX IV Laboratory, Lund University, PO Box 118, S-221 00 Lund, Sweden., Ward C; MAX IV Laboratory, Lund University, PO Box 118, S-221 00 Lund, Sweden., Gonzalez A; MAX IV Laboratory, Lund University, PO Box 118, S-221 00 Lund, Sweden., Mueller U; MAX IV Laboratory, Lund University, PO Box 118, S-221 00 Lund, Sweden.
Jazyk: angličtina
Zdroj: Journal of synchrotron radiation [J Synchrotron Radiat] 2020 Sep 01; Vol. 27 (Pt 5), pp. 1415-1429. Date of Electronic Publication: 2020 Aug 05.
DOI: 10.1107/S1600577520008723
Abstrakt: BioMAX is the first macromolecular crystallography beamline at the MAX IV Laboratory 3 GeV storage ring, which is the first operational multi-bend achromat storage ring. Due to the low-emittance storage ring, BioMAX has a parallel, high-intensity X-ray beam, even when focused down to 20 µm × 5 µm using the bendable focusing mirrors. The beam is tunable in the energy range 5-25 keV using the in-vacuum undulator and the horizontally deflecting double-crystal monochromator. BioMAX is equipped with an MD3 diffractometer, an ISARA high-capacity sample changer and an EIGER 16M hybrid pixel detector. Data collection at BioMAX is controlled using the newly developed MXCuBE3 graphical user interface, and sample tracking is handled by ISPyB. The computing infrastructure includes data storage and processing both at MAX IV and the Lund University supercomputing center LUNARC. With state-of-the-art instrumentation, a high degree of automation, a user-friendly control system interface and remote operation, BioMAX provides an excellent facility for most macromolecular crystallography experiments. Serial crystallography using either a high-viscosity extruder injector or the MD3 as a fixed-target scanner is already implemented. The serial crystallography activities at MAX IV Laboratory will be further developed at the microfocus beamline MicroMAX, when it comes into operation in 2022. MicroMAX will have a 1 µm × 1 µm beam focus and a flux up to 10 15  photons s -1 with main applications in serial crystallography, room-temperature structure determinations and time-resolved experiments.
(open access.)
Databáze: MEDLINE
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