Evaluation of setting time and compressive strength of a new bone cement precursor powder containing Mg-Na-Ca.

Autor: Esnaashary MH; School of Metallurgy and Materials Engineering, Iran University of Science and Technology, Tehran, Iran., Rezaie HR; School of Metallurgy and Materials Engineering, Iran University of Science and Technology, Tehran, Iran., Khavandi A; School of Metallurgy and Materials Engineering, Iran University of Science and Technology, Tehran, Iran., Javadpour J; School of Metallurgy and Materials Engineering, Iran University of Science and Technology, Tehran, Iran.
Jazyk: angličtina
Zdroj: Proceedings of the Institution of Mechanical Engineers. Part H, Journal of engineering in medicine [Proc Inst Mech Eng H] 2018 Oct; Vol. 232 (10), pp. 1017-1024. Date of Electronic Publication: 2018 Sep 07.
DOI: 10.1177/0954411918796048
Abstrakt: Taking the advantage of a novel magnesium phosphate precursor containing Na and Ca, the cementation rate of the cement, including only Mg/Mg-Na-Ca, was studied. Besides, two effective parameters, that is, calcination temperature, 650 °C and 800 °C, and powder-to-cement liquid ratio, 1 and 1.5 g/mL, were assessed. X-ray diffraction, scanning electron microscopy, ion chromatography, particle size analyser, Vicat needle and compression test were used to characterize the powders and obtained cements. The sample containing Mg-Na-Ca, calcined at 800 °C with powder-to-cement liquid ratio of 1.5, obtained the highest compressive strength, 20 MPa, but set fast. To control the kinetics of cementation, the powder containing Mg-Na-Ca calcined at 950 °C with powder-to-cement liquid ratio of 1.5 and 2 g/mL was assessed and the one with 2 g/mL set in 9 min possessing 22 MPa compressive strength was selected as optimal condition to be used as a candidate, injectable bone cement.
Databáze: MEDLINE