Autor: |
Dachavaram SS; Department of Pharmaceutical Sciences College of Pharmacy, University of Arkansas for Medical Sciences, Little Rock, AR 72205, USA. PACrooks@uams.edu., Penthala NR, Calahan JL, Munson EJ, Crooks PA |
Jazyk: |
angličtina |
Zdroj: |
Organic & biomolecular chemistry [Org Biomol Chem] 2018 Aug 22; Vol. 16 (33), pp. 6057-6062. |
DOI: |
10.1039/c8ob01438h |
Abstrakt: |
A mild, efficient and rapid protocol was developed for the deprotection of alcoholic TBDMS ethers using a recyclable, eco-friendly highly sulphated cellulose sulphate acid catalyst in methanol. This acid catalyst selectively cleaves alcoholic TBDMS ethers in bis-TBDMS ethers containing both alcoholic and phenolic TBDMS ether moieties. |
Databáze: |
MEDLINE |
Externí odkaz: |
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