4-Meth-oxy-N-[(4-methyl-phen-yl)sulfon-yl]benzamide including an unknown solvate.

Autor: Sreenivasa S; Department of Studies and Research in Chemistry, Tumkur University, Tumkur, Karnataka 572 103, India., Palakshamurthy BS; Department of Studies and Research in Physics, U.C.S., Tumkur University, Tumkur, Karnataka 572 103, India., Tonannavar J; Department of Physics, Karnatak University, Dharwad, Karnataka 580 003, India., Jayashree Y; Department of Physics, Karnatak University, Dharwad, Karnataka 580 003, India., Sudha AG; University College of Science, Tumkur University, Tumkur, India., Suchetan PA; Department of Studies and Research in Chemistry, U.C.S., Tumkur University, Tumkur, Karnataka 572 103, India.
Jazyk: angličtina
Zdroj: Acta crystallographica. Section E, Structure reports online [Acta Crystallogr Sect E Struct Rep Online] 2013 Oct 19; Vol. 69 (Pt 11), pp. o1664-5. Date of Electronic Publication: 2013 Oct 19 (Print Publication: 2013).
DOI: 10.1107/S1600536813028158
Abstrakt: In the title compound, C15H15NO4S, the dihedral angle between the benzene rings is 78.62 (16)°. In the crystal, adjacent mol-ecules are linked along the c axis into C(4) chains through strong N-H⋯O hydrogen bonds. Mol-ecules are further connected through C-H⋯O hydrogen bonds into a hexa-meric unit generating an R (6) 6(66) motif. Another C-H⋯O inter-action connects the mol-ecules along the c axis, forming C(5) chains. A region of disordered electron density, most probably disordered methanol-water solvent mol-ecules, was treated with the SQUEEZE routine in PLATON [Spek (2009 ▶). Acta Cryst. D65, 148-155]. The formula mass and unit-cell characteristics do not take into account this disordered solvent.
Databáze: MEDLINE