| Autor: |
Moorhouse SJ; Chemistry Research Laboratory, University of Oxford, Mansfield Road, Oxford OX1 3TA, United Kingdom., Vranješ N, Jupe A, Drakopoulos M, O'Hare D |
| Jazyk: |
angličtina |
| Zdroj: |
The Review of scientific instruments [Rev Sci Instrum] 2012 Aug; Vol. 83 (8), pp. 084101. |
| DOI: |
10.1063/1.4746382 |
| Abstrakt: |
A versatile, infrared-heated, chemical reaction cell has been assembled and commissioned for the in situ study of a range of chemical syntheses using time-resolved energy-dispersive X-ray diffraction (EDXRD) on Beamline I12 at the Diamond Light Source. Specialized reactor configurations have been constructed to enable in situ EDXRD investigation of samples under non-ambient conditions. Chemical reactions can be studied using a range of sample vessels such as alumina crucibles, steel hydrothermal autoclaves, and glassy carbon tubes, at temperatures up to 1200 °C. |
| Databáze: |
MEDLINE |
| Externí odkaz: |
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