2-[1-(2-Hydr-oxy-3-methoxy-benz-yl)-1H-benzimidazol-2-yl]-6-methoxy-phenol methanol 1.13-solvate.

Autor: Al-Douh MH, Osman H, Hamid SA, Kia R, Fun HK
Jazyk: angličtina
Zdroj: Acta crystallographica. Section E, Structure reports online [Acta Crystallogr Sect E Struct Rep Online] 2009 Mar 31; Vol. 65 (Pt 4), pp. o925-6. Date of Electronic Publication: 2009 Mar 31.
DOI: 10.1107/S1600536809011192
Abstrakt: In the main mol-ecule of the title compound, C(22)H(20)N(2)O(4)·1.13CH(4)O, the dihedral angles between the benzimidazole plane and the two benzene rings are 80.53 (10) and 82.76 (10)°. The solvent mol-ecules are disordered between three positions, with refined occupancies of 0.506 (13), 0.373 (13) and 0.249 (5). The crystal structure is stabilized by inter-molecular O-H⋯O, O-H⋯N and C-H⋯O hydrogen bonds. The crystal studied was a merohedral twin [BASF ratio of 0.917 (1)/0.083 (1)].
Databáze: MEDLINE