1-(2-Nitro-phen-yl)-3-phenyl-thio-urea.

Autor: Qin Y; New Materials & Function Coordination Chemistry Laboratory, Qingdao University of Science & Technology, Qingdao, 266042, People's Republic of China., Jian F, Jiang M, Yang X
Jazyk: angličtina
Zdroj: Acta crystallographica. Section E, Structure reports online [Acta Crystallogr Sect E Struct Rep Online] 2007 Dec 06; Vol. 64 (Pt 1), pp. o142. Date of Electronic Publication: 2007 Dec 06.
DOI: 10.1107/S1600536807063374
Abstrakt: The title compound, C(13)H(11)N(3)O(2)S, was prepared by reaction of 2-nitro-benzenamine, KOH and 1-isothio-cyanato-benzene in an ethanol solution at room temperature. The dihedral angles formed between the thiourea plane and the phenyl rings are 61.9 and 31.0°. The dihedral angle between the two phenyl rings is 78.1°. In the crystal structure, there are weak inter-molecular N-H⋯S and C-H⋯S hydrogen-bonding inter-actions.
Databáze: MEDLINE