| Autor: |
Shevchenko VP; Institute of Molecular Genetics, Russian Academy of Sciences, pl. Kurchatova 2, Moscow, 123182 Russia. nagaev@img.ras.ru, Nagaev IIu, Levina IS, Kulikova LE, Miasoedov NF, Kamernitzkiĭ AV |
| Jazyk: |
ruština |
| Zdroj: |
Bioorganicheskaia khimiia [Bioorg Khim] 2010 Mar-Apr; Vol. 36 (2), pp. 283-8. |
| DOI: |
10.1134/s1068162010020172 |
| Abstrakt: |
1,2-Tritium-labeled 3-(O-carboxypropyl)- and 3-(O-carbomethoxypropyl)-oximes of 6alpha-methyl-16alpha,17alpha-cyclohexanopregn-4-ene-3,20-diones were obtained by the homogeneous catalytic hydrogenation of 1,2-dehydroprecursors with gaseous tritium and the subsequent separation of the resulting mixtures by HPLC. The specific radioactivities of 50-55 Ci/mmol were prepared using tris-(triphenylphosphine)-rhodium chloride. |
| Databáze: |
MEDLINE |
| Externí odkaz: |
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