NMR and conformational studies of new 5-phenylpyrrole-carboxamide derivatives.
| Autor: | López-Cara LC; Departamento de Química Farmacéutica y Orgánica, Facultad de Farmacia, Universidad de Granada, 18071 Granada, Spain., Pineda de las Infantas MJ, Carrión MD, Camacho ME, Gallo MA, Espinosa A, Entrena A |
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| Jazyk: | angličtina |
| Zdroj: | Magnetic resonance in chemistry : MRC [Magn Reson Chem] 2009 Dec; Vol. 47 (12), pp. 1101-9. |
| DOI: | 10.1002/mrc.2524 |
| Abstrakt: | The 1H and 13C NMR resonances of 22 5-(5-substituted-2-nitrophenyl)-1H-pyrrole-2-carboxamides, 22 5-(5-substituted-2-aminophenyl)-1H-pyrrole-2-carboxamides, and 9 5-phenyl-1H-pyrrole-2-carboxamides were assigned completely using the concerted application of one- and two-dimensional experiments (DEPT, gs-HMQC and gs-HMBC). NOE studies and conformational analysis confirm the preferred conformations of such compounds. (Copyright 2009 John Wiley & Sons, Ltd.) |
| Databáze: | MEDLINE |
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