Autor: |
Arai T; Department of Molecular Probes, Molecular Imaging Center, National Institute of Radiological Sciences, 4-9-1 Anagawa, Inage-ku, Chiba 263-8555, Japan., Zhang MR, Ogawa M, Fukumura T, Kato K, Suzuki K |
Jazyk: |
angličtina |
Zdroj: |
Applied radiation and isotopes : including data, instrumentation and methods for use in agriculture, industry and medicine [Appl Radiat Isot] 2009 Feb; Vol. 67 (2), pp. 296-300. Date of Electronic Publication: 2008 Oct 08. |
DOI: |
10.1016/j.apradiso.2008.09.013 |
Abstrakt: |
[1-(11)C]Acetyl chloride ([(11)C]AcCl), an important [(11)C]acylating agent, was synthesized by reacting [(11)C]CO(2) with methylmagnesium bromide coated on the inner surface of a polyethylene loop (loop method). By optimizing the reaction conditions and synthesis parameters, [1-(11)C]phenylacetate and [1-(11)C]benzylacetate were produced from [(11)C]AcCl in high radiochemical yield and specific activity. |
Databáze: |
MEDLINE |
Externí odkaz: |
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