| Autor: |
Rodziewicz L; Pracownia Badań Chemicznych Srodków Spozywczych, Zakład Higieny Weterynaryjnej 15-959 Białystok, ul. Zwyciestwa 26a. rodziewicz@wiw.bianet.com.pl, Zawadzka I |
| Jazyk: |
polština |
| Zdroj: |
Roczniki Panstwowego Zakladu Higieny [Rocz Panstw Zakl Hig] 2007; Vol. 58 (3), pp. 503-8. |
| Abstrakt: |
Chloropromazina (CP) is subjected to monitoring food animals products, with a minimum required performance limit (MPRL) set 5.0 microg/kg. Homogenized kidney and urine were extracted with acetonitrile. CP- d3 was used as internal standard. LC separation was done on Luna C18 150 x 2 mm, 5 microm column in mobile phase acetonitrile-acetic acid. CP was determination by LC-ESI-MS/MS negative mode. The method was validation according to the criteria of Decision Commission No 2002/657/EC. Recoveries for the level 5.0 ng/g were in the range 84-102%. The limit of decision (CCalpha) and detection capability (CCbeta) CP in kidney were 1.19; 2.87 ng/g and urine 1.08; 2.61 ng/g. |
| Databáze: |
MEDLINE |
| Externí odkaz: |
|
