| Autor: |
Schulz K; Institut für Rechtsmedizin, Technische Universität Dresden, Fetscherstr. 74, D-01307 Dresden, Germany., Dressler J, Sohnius EM, Lachenmeier DW |
| Jazyk: |
angličtina |
| Zdroj: |
Journal of chromatography. A [J Chromatogr A] 2007 Mar 23; Vol. 1145 (1-2), pp. 204-9. Date of Electronic Publication: 2007 Jan 27. |
| DOI: |
10.1016/j.chroma.2007.01.082 |
| Abstrakt: |
The use of headspace adsorbent traps in combination with gas chromatography was evaluated for the determination of volatile constituents (i.e. higher alcohols and other congeners of alcoholic fermentation) in spirits. The headspace trap technology comprises an enhanced static headspace system that allows enrichment and focusing of analytes on adsorbent traps prior to gas chromatographic separation. Extraction yields 35-55 times higher than those seen with static headspace sampling were achieved. An excellent agreement of analysis results in comparison to the European reference procedure was found (R>0.98, p<0.0001). The fully automated headspace trap procedure requires only minimal sample preparation and is easy to apply. |
| Databáze: |
MEDLINE |
| Externí odkaz: |
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