Crystal structure of 2,3-dimethoxy-5,6,7,8,13,13a-hexahydro-6a,8-diazaindeno[2,1-b]phenanthrene methanol monosolvate
| Autor: | Shahobiddin M. Adizov, Abdusalom Sh. Saidov, Kambarali K. Turgunov, Rasul Ya. Okmanov, Bakhodir Tashkhodjaev |
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| Jazyk: | angličtina |
| Rok vydání: | 2015 |
| Předmět: | |
| Zdroj: | Acta Crystallographica Section E: Crystallographic Communications, Vol 71, Iss 8, Pp o574-o575 (2015) |
| Druh dokumentu: | article |
| ISSN: | 2056-9890 20569890 |
| DOI: | 10.1107/S2056989015013286 |
| Popis: | The asymmetric unit of the title solvate, C21H22N2O2·CH3OH, contains one methanol solvent molecule and one molecule of the heterocycle that is built up by the fusion of four six-membered rings A, C, D, E and one five-membered ring B. The indole moiety (rings A and B) is essentially planar, with an r.m.s. deviation of 0.013 Å, whereas rings C and D adopt a twisted conformation with a trans-ring junction. In the crystal, two heterocyclic molecules are associated with two methanol molecules through mutual N—H...O and O—H...N hydrogen bonds, forming a centrosymmetric dimer. |
| Databáze: | Directory of Open Access Journals |
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